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廠家對nd鋼管一般斑點(diǎn)狀偏析(xī)成因解決(jué)方法

發布時間:2019-05-20人氣:443

對ND鋼管一般斑點狀偏析的成因分析:根據試驗分析,結合(hé)nd鋼管鍛造生產情況(kuàng),在排除一般疏鬆、氣體過飽和、鋼液純淨度太差等(děng)因素後,通過金相及能譜分析,發(fā)現點偏處組織有別於基體組織,如晶(jīng)粒細化,硬度偏高(達310~340HV),組織也非(fēi)珠光體正常組織,從(cóng)而認為現有(yǒu)的點偏缺陷實質(zhì)是受合金(jīn)成分(fèn)偏析(xī)導致的組織(zhī)偏析。
Analysis of the causes of the general speckle segregation of ND steel pipes: According to the experimental analysis and combined with the forging production of ND steel pipes, after excluding the factors such as general porosity, gas supersaturation and poor purity of molten steel, metallographic and energy spectrum analysis showed that the structure at the point deviation was different from the matrix structure, such as grain refinement, high hardness (310-340HV), and the structure was not normal pearlite structure. It is believed that the existing point segregation defect is essentially the segregation of the structure caused by the segregation of the alloy composition. 酸浸塔形分析:將帶點偏缺(quē)陷(xiàn)的nd鋼管(guǎn)改鍛成Φ210mm,取Φ210mm×200mm樣坯車(chē)削成4級等長台階(jiē)(一級(jí)Φ150mm,二(èr)級Φ130mm,三(sān)級Φ110mm,四級Φ90mm),做酸(suān)浸塔形檢(jiǎn)測,在鍛材Φ110mm、Φ90mm兩級台(tái)階上發現明顯的類似於墊片的縱向暗條,而(ér)Φ150mm,Φ130mm兩級台階(jiē)上縱向暗條紋則不明顯。
Acid leaching tower shape analysis: the ND steel pipe with point deviation defect was forged into 210 mm, and the sample blank of 210 mm * 200 mm was turned into four equal-length steps (first 150 mm, second 130mm, third 110 mm, fourth 90 mm). The acid leaching tower shape detection was carried out. The vertical dark stripes similar to gaskets were found on the forged steel 110 mm and 90 mm steps, while the vertical dark stripes on the two steps of 150 mm and 90 mm were found. It is not obvious.

氣體檢測:根(gēn)據所收(shōu)集的(de)5爐鋼相關(guān)氣體的檢測數據發現,點(diǎn)偏的出現及級(jí)別與nd鋼管中氣(qì)體含(hán)量並無(wú)直接關係。
Gas Detection: According to the collected data of gas related to 5 stoves of steel, it is found that the occurrence and grade of point deviation is not directly related to the gas content in ND steel pipe.

金相分析:在酸洗過(guò)的低倍試樣上(shàng)點偏(piān)缺陷密集部位切取金相試樣進行高倍(bèi)分(fèn)析(xī);對nd鋼管試樣進行拋光(guāng)、高倍輕腐蝕後觀察宏觀形貌;將試樣偏析部位(wèi)標(biāo)識後再次進行低倍酸浸重腐蝕(shí)試驗。上述金相分析(xī)結果表(biǎo)明(míng),偏析區組織類似於貝氏體組織,基(jī)體為珠光體+鐵素體;掃描電鏡下觀察,組織明顯存在不均勻,進一步放大倍數觀察,通過對(duì)點偏(piān)缺陷位(wèi)置處能譜(pǔ)分析,發現了以MnS為代表的夾雜物的偏聚。
Metallographic analysis: metallographic specimens were cut at the point defect-intensive part of pickled low-power specimens for high-power analysis; ND steel tube specimens were polished and observed after high-power light corrosion; the segregation parts of the specimens were marked and the heavy corrosion test of low-power acid leaching was carried out again. The metallographic analysis results show that the segregation zone is similar to bainite structure, and the matrix is pearlite + ferrite. The structure is obviously inhomogeneous under scanning electron microscopy, and further magnification observation. The segregation of inclusions represented by MnS is found by energy spectrum analysis at the locations of the point deviation defect.

結合上述分析結果,排除了點(diǎn)偏為一般疏鬆誤判(pàn)的可能,也排除了由於氣體過飽和所引起的nd鋼管點狀偏析的可能,還排除了鋼液純淨度太(tài)差,夾雜物偏聚所(suǒ)致形成點狀偏析的可(kě)能。
Combined with the above analysis results, the possibility of misjudgement of point deviation for general looseness is excluded, the possibility of point segregation for ND steel tube caused by gas supersaturation is also excluded, and the possibility of point segregation caused by poor purity of molten steel and inclusion segregation is also excluded.


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